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MALDI MS spectrum of a decasaccharide D3 digestion mixture after a 270-min incubation with heparinase I. P refers to the protonated peptide (arg-gly)15. SOS, T5, H8, O11, and D3 refer to protonated complexes of peptide with sucrose octasulfate and with the oligosaccharide substrates and products (Table 1). Complexes shown in brackets were not detected. Adducts are indicated by asterisks as in the accompanying paper by Rhomberg et al. (14).
