Table 2.
Carbon no. | 13C shift (δ), ppm | 1H shift (δ), ppm |
---|---|---|
1 | 175.5 | |
2 | 44.8 | 2.93 |
3 | 80.7 | 3.79 |
4 | 37.6 | 1.93 |
5 | 81.6 | 3.86 |
6 | 76.7 | |
7 | 38.4 | 1.72, 193 |
8 | 44.7 | 2.70 |
9 | 222.4 | |
10 | 37.7 | 3.01 |
11 | 68.9 | 3.82 |
12 | 74.4 | |
13 | 76.7 | 5.06 |
14 | 21.2 | 1.47, 1.91 |
15 | 10.7 | 0.84 |
2-CH3 | 15.9 | 1.29 |
4-CH3 | 9.7 | 1.14 |
6-CH2-CH3 | 27.6 | 1.70, 2.02 |
6-CH2-CH3 | 7.7 | 0.98 |
8-CH3 | 18.6 | 1.17 |
10-CH3 | 12.3 | 3.01 |
12-CH3 | 68.9 | 3.82 |
1′ | 102.5 | 4.48 |
2′ | 72.5 | 3.21 |
3′ | 65.3 | 2.44 |
4′ | 28.3 | 1.22, 1.63 |
5′ | 68.7 | 3.52 |
6′ | 21.6 | 1.22 |
3′-N(CH3)2 | 40.7 | 2.29 |
1" | 96.2 | 4.92 |
2" | 35.3 | 2.34, 1.66 |
3" | 72.4 | |
4" | 77.7 | 3.02 |
5" | 66.3 | 3.98 |
6" | 21.6 | 1.29 |
3"-OCH3 | 49.7 | 3.33 |
3"-CH3 | 21.4 | 1.26 |
Numbering of carbon atoms of Er is as described (17).