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The amide proton region of 1-D NMR experiments of HKP1 in the presence of increasing concentrations of deuterated DPC (dDPC). The initial spectrum in the absence of detergent shows a single amide resonance and side-chain resonances. Minimal chemical dispersion consistent with an unstructured peptide. In the presence of 100 mM dDPC, the region shows increased chemical shift dispersion, consistent with the peptide adopting a defined structure.
