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. 2004 Jan;13(1):145–154. doi: 10.1110/ps.03352504

Table 1B.

Kinetic constants for cleavage of the fluorogenic substrate Ala-Pro-AFC and the chromogenic substrate Gly-Pro-pNA by wild-type DPPIV and DPPIV glycosylation mutants (proteins expressed in Hi5 insect cells)

DPPIV mutant Km (μM) kcat (s−1) kcat/Km (M−1 s−1) Relative kcat/Km
Kinetic constants for cleavage of Ala-Pro-AFC
    Wild-type DPPIV 16 23 1.4 × 106 1.0
    DPPIV-N85A 16 27 1.7 × 106 1.2
    DPPIV-N92A 17 31 1.9 × 106 1.4
    DPPIV-N150A 17 37 2.2 × 106 1.6
    DPPIV-N219A 19 42 2.2 × 106 1.6
    DPPIV-N229A 15 40 2.7 × 106 1.9
    DPPIV-N281A 20 40 2.0 × 106 1.4
    DPPIV-N321A 18 34 1.8 × 106 1.3
    DPPIV-N520A 17 36 2.1 × 106 1.5
    DPPIV-N685A 15 30 1.9 × 106 1.4
Kinetic constants for cleavage of Gly-Pro-pNA
    Wild-type DDPIV 138 24 1.7 × 105 1.0
    DPPIV-N85A 149 30 2.0 × 105 1.2
    DPPIV-N92A 143 34 2.4 × 105 1.4
    DPPIV-N150A 151 40 2.6 × 105 1.5
    DPPIV-N219A 160 45 2.8 × 105 1.6
    DPPIV-N229A 145 43 3.0 × 105 1.8
    DPPIV-N281A 168 43 2.5 × 105 1.5
    DPPIV-N321A 146 35 2.4 × 105 1.4
    DPPIV-N520A 131 35 2.7 × 105 1.6
    DPPIV-N685A 142 32 2.2 × 105 1.3