Table 4. Data-collection statistics.
Values in parentheses are for the last (highest) resolution shell.
Native data (with Mg2+) | |
---|---|
Wavelength (Å) | 1.0000 |
Space group | C2221 |
Unit-cell parameters (Å) | a = 160.15, b = 180.47, c = 57. 98 |
Resolution range (Å) | 48–1.85 (1.93–1.85) |
No. of observed reflections | 355151 |
No. of unique reflections | 72065 (8212) |
Completeness (%) | 99.9 (100) |
Multiplicity | 4.9 (4.9) |
Rmerge† | 0.090 (0.540) |
Rmeas‡ | 0.066 (0.584) |
I/σ(I) | 14.62 (2.98) |
Solvent content (%) | 58.9 |
R
merge = /
, where I
h,i is the ith observation of reflection h and 〈Ih〉 is its mean intensity.
R
meas =
, where I
h,i is the ith observation of reflection h and nh is the multiplicity.