Table 1. X-ray diffraction data statistics of DHNA synthetase.
Wavelength (Å) | 1.0 |
Space group | C2221 |
Temperature (K) | 100 |
Unit-cell parameters (Å) | a = 77.01, b = 130.66, c = 131.69 |
Matthews coefficient (Å3 Da−1) | 1.83 (3 subunits per ASU) |
Solvent content (%) | 32.8 |
Resolution range (Å) | 50.0–2.20 (2.28–2.20) |
No. of observed reflections | 1320862 |
No. of unique reflections | 33813 (3181) |
Completeness (%) | 98.9 (94.2) |
Rsym† (%) | 4.1 (8.1) |
Multiplicity | 9.8 (6.5) |
Average I/σ(I) | 39 (14) |
R sym = .