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. 2007 Jan 17;63(Pt 2):103–105. doi: 10.1107/S1744309106056521

Table 1. X-ray diffraction data statistics of DHNA synthetase.

Values in parentheses are for the last resolution bin.

Wavelength (Å) 1.0
Space group C2221
Temperature (K) 100
Unit-cell parameters (Å) a = 77.01, b = 130.66, c = 131.69
Matthews coefficient (Å3 Da−1) 1.83 (3 subunits per ASU)
Solvent content (%) 32.8
Resolution range (Å) 50.0–2.20 (2.28–2.20)
No. of observed reflections 1320862
No. of unique reflections 33813 (3181)
Completeness (%) 98.9 (94.2)
Rsym (%) 4.1 (8.1)
Multiplicity 9.8 (6.5)
Average I/σ(I) 39 (14)

R sym = Inline graphic Inline graphic.