Table 1. Data-collection statistics.
Values in parentheses are for the highest resolution shell.
| BPL* | BPL** | BCCPΔN76 | BPL*–BCCPΔN76 | BPL**–BCCPΔN76 | |
|---|---|---|---|---|---|
| Space group | P21 | P21 | P212121 | P21 | P21 |
| Unit-cell parameters (Å) | |||||
| a (Å) | 38.36 | 38.30 | 39.69 | 69.57 | 69.85 |
| b (Å) | 82.77 | 82.88 | 39.77 | 63.48 | 63.12 |
| c (Å) | 72.71 | 72.58 | 88.42 | 75.72 | 75.64 |
| β (°) | 103.2 | 103.5 | 90.0 | 93.7 | 95.9 |
| VM (Å3 Da−1) | 2.16 | 2.15 | 2.18 | 2.45 | 2.45 |
| Wavelength (Å) | 1.00000 | 1.00000 | 1.00000 | 1.00000 | 1.00000 |
| Resolution range (Å) | 50–1.45 (1.50–1.45) | 50–1.50 (1.55–1.50) | 50–1.55 (1.61–1.55) | 50–2.70 (2.80–2.70) | 50–2.00 (2.07–2.00) |
| Total observations | 224041 | 244726 | 123723 | 47075 | 133241 |
| Unique reflections | 72231 | 69164 | 20755 | 15564 | 42152 |
| Multiplicity | 3.2 (2.9) | 3.6 (3.3) | 6.0 (3.4) | 3.1 (2.8) | 3.2 (3.0) |
| Completeness (%) | 92.4 (97.2) | 98.1 (95.9) | 98.5 (98.0) | 95.1 (86.6) | 95.8 (90.0) |
| Mean I/σ(I) | 15.5 (3.1) | 12.8 (2.2) | 27.7 (3.1) | 6.9 (2.0) | 9.0 (2.8) |
| Rmerge† (%) | 4.8 (37.9) | 4.2 (27.4) | 4.5 (29.2) | 10.7 (32.0) | 8.7 (31.3) |
†
R
merge = 
, where Ij(hkl) and 〈I(hkl)〉 are the observed intensity of measurement j and the mean intensity of the reflection with indices hkl, respectively.