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. Author manuscript; available in PMC: 2008 Apr 24.
Published in final edited form as: Tetrahedron Lett. 2007 Nov 5;48(45):8029–8033. doi: 10.1016/j.tetlet.2007.09.037

Table 2.

Preparation of N-hydroxysulfamides 3

graphic file with name nihms32945t3.jpg
Entry Substrate Product R Yielda (%)
1 1c 3a Bn H 93
2 1d 3b c-hexyl H 90
3 2a 3c CH3 CH3CH2 97
4 2d 3d CH3 graphic file with name nihms32945t4.jpg 85
a)

two-step yield