Table 2.
Preparation of N-hydroxysulfamides 3
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|---|---|---|---|---|---|
| Entry | Substrate | Product | R | R¹ | Yielda (%) |
| 1 | 1c | 3a | Bn | H | 93 |
| 2 | 1d | 3b | c-hexyl | H | 90 |
| 3 | 2a | 3c | CH3 | CH3CH2 | 97 |
| 4 | 2d | 3d | CH3 | 85 | |
two-step yield
Preparation of N-hydroxysulfamides 3
![]() | |||||
|---|---|---|---|---|---|
| Entry | Substrate | Product | R | R¹ | Yielda (%) |
| 1 | 1c | 3a | Bn | H | 93 |
| 2 | 1d | 3b | c-hexyl | H | 90 |
| 3 | 2a | 3c | CH3 | CH3CH2 | 97 |
| 4 | 2d | 3d | CH3 | 85 | |
two-step yield