Table 1. Data-collection statistics of HLA-B*1402–pLMP2 and HLA-B*1402–pCatA.
HLA-B*1402–pLMP2 | HLA-B*1402–pCatA | |
---|---|---|
Space group | P21 | P212121 |
Unit-cell parameters (Å) | a = 53.4, b = 79.9, c = 105.4, α = 90, β = 99.5, γ = 90 | a = 50.8, b = 82.1, c = 110.7, α = 90, β = 90, γ = 90 |
Solvent content (%) | 50.2 | 52.2 |
Matthews coefficient† (Å3 Da−1) | 2.5 | 2.6 |
Resolution (Å) | 30.0–2.55 (2.64–2.55) | 50.0–1.86 (1.93–1.86) |
Unique reflections | 26733 (2177) | 38359 (3023) |
Completeness (%) | 93.0 (76.8) | 96.8 (78.0) |
〈I〉/〈σ(I)〉 | 7.9 (1.4) | 22.5 (3.5) |
Rsym‡ | 0.137 (0.457) | 0.049 (0.239) |
Rmerge§ | 0.138 (0.449) | 0.073 (0.247) |
Rr.i.m.§ | 0.165 (0.585) | 0.082 (0.294) |
Rp.i.m.§ | 0.089 (0.371) | 0.036 (0.155) |
Redundancy | 3.0 (1.8) | 4.6 (2.7) |