Table 1. Crystal data and data-collection statistics.
Space group | P3121 |
Unit-cell parameters (Å) | a = b = 92.4, c = 114.3 |
No. of protomers per ASU | 1 |
X-ray source | BL41XU, SPring-8 |
Temperature (K) | 100 |
Wavelength (Å) | 1.0000 |
Oscillation range (°) | 1.0 |
Crystal-to-detector distance (mm) | 400 |
No. of frames | 180 |
Resolution range (Å) | 100–3.30 (3.48–3.30) |
Observed reflections | 91781 |
Unique reflections | 8884 |
Completeness (%) | 100 (100) |
Multiplicity | 10.3 (10.7) |
Mean I/σ(I) | 5.4 (1.4) |
Rmerge† | 0.106 (0.540) |
R merge = , where 〈I〉h is the mean intensity of symmetry-equivalent reflections.