Table 1. X-ray data-collection statistics.
Values in parentheses are for the outer shell.
| Resolution (Å) | 50–1.74 (1.80–1.74) |
| Wavelength (Å) | 1.0 |
| Data-collection temperature (K) | 110 |
| No. of observed reflections | 1018072 |
| No. of unique reflections | 55192 |
| Completeness (%) | 99.1 (93.5) |
| Mean I/σ(I) | 13.9 (2.14) |
| Rsym† (%) | 12.0 (83.1) |
R
sym =
.