Table 2.
entry | D | A | time | product | yield, % | α/β ratio |
---|---|---|---|---|---|---|
1 | 3a | 20 | 10 min | 21 | 86 | 1.1/1 |
2 | 4a | 20 | 20 min | 21 | 85 | 3.3/1 |
3 | 5a | 20 | 10 min | 21 | 83 | 1/1.2 |
4 | 9 | 20 | 16 h | 21 | 65a | 1.6/1 |
5 | 2a | 22 | 15 min | 23 | 84 | 1.6/1 |
6 | 3a | 22 | 20 min | 23 | 87 | 2.0/1 |
7 | 5a | 22 | 15 min | 23 | 89 | 2.4/1 |
8 | 8 | 22 | 15 min | 23 | 84 | 2.2/1 |
9 | 9 | 22 | 24 h | 23 | 83a | 2.4/1 |
the yield is based on the recovered acceptor