Table 2.
Selected Bond Lengths (Å) and Angles (deg) for 2·4CH2Cl2·C7H8.a
| Bond length | Bond angle | ||
|---|---|---|---|
| Fe1···Fe1A | 5.173(1) | O2–Fe1–N1 | 76.08(9) |
| Fe1–N1 | 2.155(2) | O2–Fe1–N2 | 92.23(9) |
| Fe1–N2 | 2.157(2) | O2–Fe1–O7 | 164.56(8) |
| Fe1–O2 | 2.167(2) | N2–Fe1–O4 | 76.20(8) |
| Fe1–O4 | 2.154(2) | N1–Fe1–N2 | 159.45(9) |
| Fe1–O5 | 2.096(2) | O5–Fe1–O7 | 89.24(8) |
| Fe1–O7 | 2.131(2) | S1–O5–Fe1 | 133.7(1) |
| O5–S1 | 1.454(2) | O7A–S1–O5 | 112.4(1) |
| O7–S1A | 1.451(2) | ||
a
Numbers in parentheses are estimated standard deviations of the last significant figure. Atoms are labeled as indicated in Figures 3 and 4.