Table 1. Crystal data and data-collection statistics.
| X-ray source | PF BL-5A |
| Wavelength used (Å) | 1.000 |
| Space group | I222 or I212121 |
| Unit-cell parameters | |
| a (Å) | 48.13 |
| b (Å) | 60.59 |
| c (Å) | 107.21 |
| Unit-cell volume (Å3) | 312599 |
| Resolution range (Å) | 43.91–2.02 (2.09–2.02) |
| Observed reflections | 73136 |
| Unique reflections | 10628 |
| Completeness (%) | 99.99 (100.0) |
| Rmerge† (%) | 7.8 (30.9) |
| 〈I/σ(I)〉 | 11.2 (4.8) |
| Matthews coefficient (Å3 Da−1) | 2.4 |
| Solvent content (%) | 49.2 |
R
merge =
, where I(h, i) is the intensity of reflection h in the ith measurement and 〈I(h)〉 is the mean value of the intensity of reflection h.