Table 1. Data collection and refinement statistics for E81S mutant haFGF.
Data collection | |
Space group | C2221 |
Unit-cell dimensions (Å) | a = 73.5, b = 97.3, c = 108.5 |
No. of molecules per asymmetric unit | 2 |
Solvent content (%) | 58 |
Resolutions (Å) | 1.35 |
No. of observed reflections | 530712 |
No. of unique reflections | 81087 |
Redundancy | 6.5 (5.7) |
Completeness (%) | 95.0 (82.3) |
〈I/σ(I)〉 | 49.0 (4.1) |
Rmerge† | 0.043 (0.349) |
Wilson plot B factor (Å2) | 15.7 |
Refinement statistics | |
Resolutions (Å) | 20.0–1.35 |
No. of reflections | 76 990 |
R factor/Rfree‡ | 0.182/0.211 |
R.m.s.d. bonds (Å) | 0.015 |
R.m.s.d. angles (°) | 1.545 |
, where 〈I(h)〉 is the average intensity of reflection h and symmetry-related reflections.
, calculated for the reflections of the working and test (5%) sets.