TABLE 2.
Data collection and model refinement statistics
| κI O18/O8 | AL-09 | |
|---|---|---|
| Space group | P61 | P4132 |
| Cell a, b, c (Å) | 74.27, 74.27, 99.05 | 176.05 |
| Resolution (Å) | 99-1.30 (1.33-1.30)a | 176-2.55 (2.64-2.55) |
| Completeness (%) | 99.7 (96.3) | 99.3 (93.0) |
| Redundancy | 12.2 (5.6) | 98.7 (68.3) |
| Rsym | 0.046 (0.53) | 0.095 (0.47) |
| <I/σ1> | 53.2 (2.3) | 82.5 (9.8) |
| Rwork | 0.119 (0.218) | 0.165 (0.242) |
| Rfree | 0.148 (0.218) | 0.206 (0.376) |
|
No. reflections
|
74839 (5311)
|
29819 (2094)
|
| R.m.s. deviations | ||
| Bond length (Å) | 0.019 | 0.020 |
|
Bond angle (°)
|
1.78
|
1.83
|
| Ramachandran plot | ||
| Most favored regions (%) | 96.24% | 93.22% |
| Outliers (%)b | 0.00% | 0.23% |
a
Highest resolution shell shown in parenthesis
b
Ramachandran outlier for AL-09 is glycine residue 41 in chain B with phi, psi angles 37.1°, 88.4°