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. Author manuscript; available in PMC: 2009 May 18.
Published in final edited form as: Tetrahedron Lett. 2008 May 19;49(21):3496–3499. doi: 10.1016/j.tetlet.2008.03.101

Scheme 3.

Scheme 3

Synthetic approach toward tricholomalide A. Reagents and condtions: (a) TIPS-acetylene, PdCl2(PPh3)2, CuI, iPr2NH, THF, 0 °C to 23 °C, 90%. (b) KOtBu, MeI, THF, 0 °C to 23 °C, 78% (16:17 = 1:3.2).