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. Author manuscript; available in PMC: 2008 Jul 8.
Published in final edited form as: J Am Chem Soc. 2008 Jan 1;130(3):1102–1108. doi: 10.1021/ja0780075

Table 2.

Chlorins prepared by Method V

graphic file with name nihms56128f10.jpg

15 Substituentsa Yield (%) Method I Yield (%)b
a e,f = Me; g = PMe; R = Me 74 –
b e,f = Me; g = PMe; R = Ph 87 –
c e,f = Me; g = PMe; R = H 39 –
d e = Me; f,g = PMe; R = Me 78 73
e e = Me; f,g = PMe; R = Ph 73 60
f e = Me; f,g = PMe; R = H 38 63
g e = PMe; f,g = Me; R = Me 38 –
h e = PMe; f,g = Me; R = Ph 77 –
i e = PMe; f,g = Me; R = H 22 –
a

PMe = CH2CH2CO2Me.

b

see reference 21b.