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. Author manuscript; available in PMC: 2008 Aug 11.
Published in final edited form as: Inorg Chem. 2006 Jan 23;45(2):837–848. doi: 10.1021/ic051476s

Table 2.

Selected Interbond Lengths and Angles for 8a

Bond length (Å) Interbond Angle (deg)
Fe1Fe2 2.9725(11) Fe1–O2–Fe2 98.10(19)
Fe2–O3–Fe1 97.35(18)
Fe1–N1 2.210(4) O1–Fe1–N1 80.49(15)
Fe1–O1 2.023(3) O2–Fe1–N1 84.76(17)
Fe1–O2 1.954(4) O3–Fe1–N1 92.34(17)
Fe1–O3 1.981(4) O5–Fe1–N1 172.91(15)
Fe1–O5 2.003(3) O7–Fe1–N1 92.17(15)
Fe1–O7 1.947(3) O1–Fe1–O2 97.51(16)
Fe2–O2 1.981(4) O1–Fe1–O3 172.11(17)
Fe2–O3 1.977(4) O1–Fe1–O5 93.26(14)
Fe2–O4 2.097(4) O1–Fe1–O7 89.81(14)
Fe2–O6 2.017(3) O2–Fe1–O3 78.40(17)
Fe2–O9 1.974(3) O2–Fe1–O5 92.81(17)
Fe2–O11 1.976(3) O2–Fe1–O7 171.47(17)
O3–Fe1–O5 93.68(16)
O2O10 2.708(6) O3–Fe1–O7 93.80(16)
O3O8 2.803(6) O5–Fe1–O7 91.14(14)
O4O12 2.537(6) O2–Fe2–O3 77.85(17)
O2–Fe2–O4 89.52(19)
O2–Fe2–O6 91.58(16)
O2–Fe2–O9 91.96(16)
O2–Fe2–O11 174.61(17)
O3–Fe2–O4 88.81(17)
O3–Fe2–O6 93.02(15)
O3–Fe2–O9 168.94(16)
O3–Fe2–O11 97.06(15)
O4–Fe2–O6 178.02(16)
O4–Fe2–O9 86.77(17)
O4–Fe2–O11 88.61(17)
O6–Fe2–O9 91.55(14)
O6–Fe2–O11 90.43(14)
O9–Fe2–O11 92.97(14)
a

Numbers in parentheses are estimated standard deviations of the last significant figure. Atoms are labeled as indicated Figures 3 and S6.