Table 4.

Crystallographic parameters of anthranilic acid derivatives

compound name	3	7	9	11	15	17	19
formula	C14H13NO2	C16H17NO2	C17H19NO2	C19H15NO2	C14H13NO2	C17H19NO2	C21H19NO2
mol wt	227.25	255.31	269.33	289.32	227.25	269.33	317.37
temp (K)	173	183	173	183	173	163	173
system	Monoclinic	Triclinic	Triclinic	Monoclinic	Triclinic	Triclinic	Triclinic
space group	C2/c	P-1	P-1	P21/c	P-1	P-1	P-1
a (Å)	11.7804(16)	7.4585(10)	7.4748(12)	5.7231(8)	4.6299(14)	10.9634(7)	10.5769(16)
b (Å)	7.4503(10)	7.5891(10)	9.3856(15)	17.929(2)	8.332(2)	11.7048(7)	11.4108(17)
c (Å)	26.627(3)	13.6653(19)	11.0319(17)	14.4300(19)	15.336(4)	22.9688(14)	14.162(2)
α(°)	90	79.998(2)	106.582(3).	90°	98.466(4)	88.8990(10)	80.856(3)
β(°)	100.168(2)	85.875(2)	91.207(3)	101.064(2)	92.198(4)	89.0970(10)	82.334(3)
γ(°)	90	62.141(2)	99.212(3)	90	101.337(4)	82.0050(10)	84.982(3)
V (Å3)	2300.3(5)	673.42(16)	730.4(2)	1453.2(3)	572.3(3)	2918.0(3)	1668.5(4)
Z	8	2	2	4	2	8	4
ρ (g/cm3)	1.312	1.259	1.225	1.322	1.319	1.226	1.263
θ range (°)	1.55–27.99	1.51–27.99	1.93–28.00	1.83–27.99	2.52–28.00	1.76–28.00	1.95–27.99
index ranges	−15 ≤ h ≤ 15	−9 ≤ h ≤ 9	−9 ≤ h ≤ 9	−7 ≤ h ≤ 7	−76≤ h ≤ 6	−14 ≤ h ≤ 14	−13 ≤ h ≤ 13
	−9 ≤ k ≤ 9	−9 ≤ k ≤ 10	−12 ≤ k ≤ 12	−23 ≤ k ≤ 22	−10 ≤ k ≤ 11	−15 ≤ k ≤ 15	−14 ≤ k ≤ 14
	−35 ≤ l ≤ 34	−17 ≤ l ≤ 18	−14 ≤ l ≤ 14	−18 ≤ l ≤ 19	−20 ≤ l ≤ 19	−30 ≤ l ≤ 29	−18 ≤ l ≤ 18
reflns collected	9959	6018	6614	12467	4861	25329	14927
unique reflns	2714	3054	3338	3401	2552	13122	7547
R(int)	0.0410	0.0282	0.0231	0.0430	0.0211	0.0345	0.0309
refined params	155	174	192	199	155	733	445
GOF on F2	1.020	0.914	1.060	1.027	0.980	1.045	1.032
R1 [I>2σ (I)]	0.0483	0.0462	0.0414	0.0463	0.0442	0.0618	0.0460
wR2 (all data)	0.1409	0.1228	0.1073	0.1127	0.1140	0.2060	0.1154