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. Author manuscript; available in PMC: 2008 Sep 18.
Published in final edited form as: J Am Chem Soc. 2007 Mar 27;129(15):4834–4839. doi: 10.1021/ja069145h

Fig 2.

Fig 2

Splittings of C2-H2 and C5-H5 of the lactose galactose residue. (A) 6mM lactose, 0.3mM Galectin-3 (pH 6.8) in 3% C12E5/Hexanol bicelle preparation doped with 0.5mM DOGS-NTA ammonium salt (no chelating metal); (B) 6mM lactose (pH 6.8) in 3% C12E5/Hexanol bicelle preparationdopedwith0.5mM DOGS-NTA-Ni; (C) 6mM lactose, 0.3mM Galectin-3 (pH 6.8) in 3% C12E5/Hexanol bicelle preparation doped with 0.5mM DOGS-NTA-Ni.