TABLE 1.
Atom no. | Carbon δC | Proton resonance
|
||
---|---|---|---|---|
δH | Multiplicity | J (Hz) | ||
1ax | 29.3 | 1.60 | ddd | 13.0, 11.5, 4.4 |
1eq | 29.3 | 1.78 | dddd | 13.5, 2.8, 2.8, 2.8 |
2 | 40.3 | 1.71 | dddd | 11, 11, 3.3, 3.3 |
3ax | 26.9 | 1.47 | dddd | 12.7, 12.7, 11.0, 3.8 |
3eq | 26.9 | 1.52 | ddddd | 12.9, 4, 4, 4, 2 |
4ax | 31.2 | 1.61 | ddd | 12.9, 12.9, 4.3 |
4eq | 31.2 | 1.08 | ddd | 13.0, 3.5, 3.5 |
4a | 31.5 | |||
5ax | 36.1 | 1.36 | ddd | 13.2, 10.9, 5.9 |
5eq | 36.1 | 1.39 | ddd | 13.1, 6.8, 2.5 |
6ax | 22.6 | 2.07 | br m | Σ Js ca. 47 |
6eq | 22.6 | 1.92 | br d | Σ Js ca. 34 |
7 | 122.7 | 5.43 | br m | Σ Js ca. 11 |
8 | 135.2 | |||
8a | 44.4 | 1.94 | br m | Σ Js ca. 13 |
9 | 150.5 | |||
10E/Z | 108.1 | 4.70 | dq | 2, 1 |
10Z/E | 108.1 | 4.69 | dq | 2, 1.5 |
11 | 21.3 | 1.73 | dd | 1.5, 1 |
12 | 27.4 | 1.00 | s | |
13 | 22.1 | 1.66 | ddd | 2.5, 1.4, 1.4 |