Table 5. Hydrogen-bond parameters (Å, °) in (II) and (III).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
| (II) | ||||
| N1—H1⋯O1 | 0.88 | 2.12 | 2.997 (1) | 177 |
| N2—H2⋯F1 | 0.86 | 1.89 | 2.721 (1) | 164 |
| (III) | ||||
| N1—H1⋯O1i | 0.80 | 2.15 | 2.921 (2) | 161 |
| N1—H2⋯F2ii | 0.90 | 2.04 | 2.908 (2) | 162 |
| N1—H3⋯F6 | 0.91 | 2.16 | 2.988 (2) | 151 |
| N1—H4⋯F1 | 0.80 | 2.01 | 2.806 (2) | 171 |
| N2—H5⋯F9 | 0.84 | 2.07 | 2.862 (1) | 158 |
| N2—H6⋯F1 | 0.80 | 2.27 | 3.000 (1) | 150 |
| N2—H7⋯O2iii | 0.94 | 2.08 | 2.986 (1) | 174 |
| N2—H8⋯F6iv | 0.88 | 1.93 | 2.806 (1) | 170 |
| N3—H9⋯F6i | 0.87 | 1.91 | 2.762 (2) | 165 |
| N3—H10⋯F7iv | 0.89 | 2.22 | 3.030 (2) | 151 |
| N3—H11⋯O2 | 0.81 | 2.11 | 2.896 (2) | 163 |
| N3—H12⋯F5v | 0.87 | 1.98 | 2.810 (2) | 157 |
| N4—H13⋯F4i | 0.87 | 2.18 | 3.036 (2) | 168 |
| N4—H14⋯F8vi | 0.84 | 2.02 | 2.835 (2) | 166 |
| N4—H15⋯F1 | 0.84 | 1.94 | 2.683 (2) | 148 |
| N4—H16⋯O1vii | 0.87 | 2.12 | 2.961 (2) | 162 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.