. Author manuscript; available in PMC: 2009 Sep 5.

Published in final edited form as: J Mol Biol. 2008 Jun 10;381(3):655–669. doi: 10.1016/j.jmb.2008.06.011

Table 1.

Summary of crystallographic data and refinement statistics.

	cGMP-bound wild type	R307E	R307W
Space Group	P2₁	P2₁	P2₁2₁2
Resolution (Å)	50.0-2.35	50.0-2.20^*	41.09-2.90
R_work (%)	20.9	20.2^*	26.0
R_free (%)	25.6	22.0^*	30.6
Rmsd bond length (Å)	0.009	0.01	0.006
Rmsd bond angle (°)	1.3	1.2	0.95
Completeness (%)	90.0 (94.0)	89.9(96.0) ^*	99.3 (97.7)
R_sym (%)	8.0 (7.9)	7.3 (28.4)	6.6 (29.6)
I/Sig I	10.0 (7.0)	8.0 (2.3)	24.0 (5.3)
Redundancy	3.3 (3.2)	4.1(2.9)	4.8 (4.6)

During refinement data included reflections to 2.0 Å. Due to outer shell incompleteness, refinement statistics and completeness are reported to 2.2 Å only.