Table 4.
Data collection | |
---|---|
Wavelength (Å) | 0.9183 |
Resolution range (Å) | 134.84-1.87 |
No. of observations | 421,119 |
No. of unique observations | 122,951 |
R unmerge (%) | 11 |
I/σ(I) | 9.0 |
Space group | C2 |
Cell dimensions (a,b,c,β) | 195.1, 78.1, 156.8, 120.4 |
Refinement | |
Resolution range (Å) | 134.84-2.2 |
Reflections | 90,926 |
Completeness (%) | 92.56 (89.9) |
R work (%) | 19.6 |
R free (%) | 27.3 |
R.m.s. deviations | |
Bond length (Å) | 0.017 |
Bond angles (°) | 1.556 |
Average B of overall | 25.82 |