Skip to main content
. Author manuscript; available in PMC: 2009 Jul 18.
Published in final edited form as: J Mol Biol. 2008 May 17;380(4):623–635. doi: 10.1016/j.jmb.2008.05.025

Table 4.

Crystallographic statistics for the A. variabilis PAL (C503S/C564S) double mutant

Data collection
  Wavelength (Å) 0.9183
  Resolution range (Å) 134.84-1.87
  No. of observations 421,119
  No. of unique observations 122,951
  R unmerge (%) 11
  I/σ(I) 9.0
  Space group C2
  Cell dimensions (a,b,c,β) 195.1, 78.1, 156.8, 120.4
Refinement
  Resolution range (Å) 134.84-2.2
  Reflections 90,926
  Completeness (%) 92.56 (89.9)
  R work (%) 19.6
  R free (%) 27.3
  R.m.s. deviations
   Bond length (Å) 0.017
   Bond angles (°) 1.556
  Average B of overall 25.82