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. Author manuscript; available in PMC: 2008 Oct 7.
Published in final edited form as: J Am Chem Soc. 2006 Apr 12;128(14):4578–4579. doi: 10.1021/ja058801v

Table 1.

Polymerization results.

Polymer [M]o/[C] Calcd./Mna PSS/Mnb Rxn Temp (°C) PDI % Yieldc
7 10/1 1796 5170 24 1.18 57
8 18/1 3149 6532 24 1.30 59
9 35/1 6025 10445 24−40 1.52 59
10 50/1 8563 16966 24−40 1.56 64
a

Number average molecular weight by NMR.

b

Number average molecular weight by GPC using polystyrene standards.

c

Isolated yield after precipitation and silica column chromatography.