Table VI.
CE-LIF percentage compositions of ΔHexAGalNAc4S, ΔHexAGalNAc6S, ΔHexA2SGalNAc4S and ΔHexA2SGalNAc6S after an exhaustive digestion of the whole DS polymer chain. Percentage Δ-disaccharide compositions were calculated using CE fluorescence peak areas normalized to the area of the internal standard.
| 1 | 2 | 3 | 4 | |
|---|---|---|---|---|
| ΔHexAGalNAc4S | ΔHexAGalNAc6S | ΔHexA2SGalNAc4S | ΔHexA2SGalNAc6S | |
| CSA | 94.65 ± 0.29 | 5.34 ± 0.02 | 0 | 0 |
| CSB | 91.10 ± 0.39 | 7.10 ± 0.03 | 1.79 ± 0.04 | 0 |
| CSC | 17.45 ± 0.17 | 78.88 ± 0.66 | 0 | 3.66 ± 0.02 |
| CS6 | 6.03 ± 0.07 | 93.97 ± 0.7 | 0 | 0 |
| DS18 | 95.51 ± 1.00 | 2.65 ± 0.13 | 1.84 ± 0.02 | 0 |
| DS36 | 94.39 ± 1.21 | 1.98 ± 0.09 | 3.69 ± 0.02 | 0 |
| DS50 | 84.16 ± 2.03 | 13.69 ± 0.27 | 2.14 ± 0.03 | 0 |
| ACD | 60.77 ± 0.25 | 39.23 ± 0.16 | 0 | 0 |
| CD | 86.75 ± 0.08 | 9.64 ± 0.01 | 3.61 ± 0.01 | 0 |
| SD | 79.39 ± 0.01 | 15.59 ± 0.01 | 5.01 ± 0.06 | 0 |