Table 1. Diffraction data statistics for Atg16 CCD crystals.
Values in parentheses are for the outer shell.
| Native | Selenomethionine | |
|---|---|---|
| Beamline | BL-5A (KEK) | BL41XU (SPring-8) |
| Wavelength (Å) | 1.1000 | 0.9791 |
| Resolution range (Å) | 50–2.70 (2.80–2.70) | 50–2.50 (2.59–2.50) |
| Observed reflections | 240090 | 640275 |
| Unique reflections | 17961 | 42101 |
| Completeness (%) | 98.8 (94.8) | 99.8 (99.9) |
| Rmerge(I)† | 0.060 (0.375) | 0.054 (0.406) |
| Mean I/σ(I) | 43.9 (4.3) | 83.4 (10.6) |
| Matthews coefficient (Å3 Da−1) | 3.17 | 3.14 |
| Wilson B factor (Å2) | 64.6 | 59.5 |
†
R
merge(I) = 
, where I
i(hkl) is the ith observed amplitude of reflection hkl and 〈I(hkl)〉 is the mean amplitude for all observed reflections.