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. 2008 Oct 28;64(Pt 11):1027–1030. doi: 10.1107/S174430910803131X

Table 1. Crystal parameters and data-collection statistics.

Values in parentheses are for the highest resolution shell.

X-ray source Synchrotron (BL44B2 at SPring-8)
Wavelength (Å) 1.0000
Detector CCD camera (ADSC Q210)
Space group P212121
Unit-cell parameters (Å)  
a 70.3
b 81.8
c 82.2
Mosaicity (°) 0.52
Wilson B factor (Å2) 15.8
Resolution range (Å) 58–2.2 (2.32–2.2)
Total observations 178036 (25785)
Unique reflections 24732 (3523)
Multiplicity 7.2 (7.3)
Completeness (%) 100.0 (100.0)
Mean I/σ(I) 12.7 (5.0)
Rmerge (%) 11.4 (42.1)

R merge = Inline graphic Inline graphic, where I i(hkl) and 〈I(hkl)〉 are the observed intensity of the ith measurement and the mean intensity of the reflection with indices hkl, respectively.