Table 1. Crystal parameters and data-collection statistics.
Values in parentheses are for the highest resolution shell.
| X-ray source | Synchrotron (BL44B2 at SPring-8) |
| Wavelength (Å) | 1.0000 |
| Detector | CCD camera (ADSC Q210) |
| Space group | P212121 |
| Unit-cell parameters (Å) | |
| a | 70.3 |
| b | 81.8 |
| c | 82.2 |
| Mosaicity (°) | 0.52 |
| Wilson B factor (Å2) | 15.8 |
| Resolution range (Å) | 58–2.2 (2.32–2.2) |
| Total observations | 178036 (25785) |
| Unique reflections | 24732 (3523) |
| Multiplicity | 7.2 (7.3) |
| Completeness (%) | 100.0 (100.0) |
| Mean I/σ(I) | 12.7 (5.0) |
| Rmerge† (%) | 11.4 (42.1) |
R
merge =
, where I
i(hkl) and 〈I(hkl)〉 are the observed intensity of the ith measurement and the mean intensity of the reflection with indices hkl, respectively.