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. Author manuscript; available in PMC: 2009 Oct 1.
Published in final edited form as: Bioorg Med Chem. 2008 Sep 9;16(19):8795–8800. doi: 10.1016/j.bmc.2008.09.016

Table 2.

1H-1H coupling constants of m4Cm and its analogues at 4, 25, and 37 °C.

Compound Temperature J1,2 J2,3 J3,4 J4,5 J4,5
C 4° C 3.8 5.1 6.3 2.8 4.3
25° C 3.9 5.3 6.1 2.8 4.4
37° C 4.0 5.4 6.1 2.9 4.5
Cm 4° C 3.3 5.2 6.8 2.6 4.2
25° C 3.5 5.3 6.7 2.8 4.4
37° C 3.5 5.4 6.5 2.8 4.4
m4C 4° C 4.3 5.4 5.5 2.8 4.4
25° C 4.4 5.4 5.6 2.9 4.6
37° C 4.4 5.4 5.6 2.9 4.6
m4Cm 4° C 3.8 5.3 6.6 2.8 4.3
25° C 3.9 5.4 6.2 2.8 4.3
37° C 3.9 5.4 6.2 2.9 4.5