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Synthesis and activation of Naphtho-Peroxyfluor-1 (NPF1). Reagents and conditions: (i) N-phenyl-bis(trifluoromethanesulfonimide), DIPEA, DMF, 25 °C, 24 h. (ii) Pd(dppf)Cl2•CH2Cl2, dppf, bis(pinacolato)diboron, KOAc, 1,4-dioxane, 100 °C, 24 h.
