Table 1.
Data collection statistics
| Crystal | Se-Met |
Native | ||
|---|---|---|---|---|
| Dataset | Peak | Edge | Remote | |
| Beamline | BL41XU (SPring-8) | BL6A (PF) | ||
| Resolution (Å) | 50–2.07 (2.14–2.07) | 50–2.07 (2.14–2.07) | 50–2.05 (2.12–2.05) | 50–2.05 (2.12–2.05) |
| Space group | C2221 | |||
| Unit cell (Å) | a = 96.0, b = 107.3, c = 105.0 | a = 95.8, b = 107.6, c = 104.8 | ||
| Wavelength (Å) | 0.9793 | 0.9796 | 0.9000 | 1.0000 |
| Unique reflections | 33233 (3123) | 33256 (3161) | 34231 (3377) | 33895 (3383) |
| Completeness (%) | 99.6 (96.8) | 99.5 (96.2) | 99.5 (99.8) | 98.7 (99.7) |
| †Rmerge (%)a | 7.5 (38.0) | 6.9 (38.6) | 6.6 (38.3) | 7.4 (38.3) |
| I/σ | 14.7 (2.5) | 16.9 (3.0) | 18.0 (3.5) | 19.6 (5.0) |
| Multiplicity | 7.1 (6.5) | 7.1 (6.3) | 7.2 (7.0) | 5.4 (5.2) |
Values in parentheses refer to the highest resolution shell †Rmerge = Σh Σj | 〈I〉h − Ihj|/Σh Σj Ihj, where 〈I〉h is the mean intensity of symmetry equivalent reflections.