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. Author manuscript; available in PMC: 2009 Feb 26.
Published in final edited form as: Biochemistry. 2008 Jan 24;47(8):2638–2649. doi: 10.1021/bi702235k

Table 3.

Quadrupolar Splittings from 2H NMR Spectra of Oriented Samples Containing WALP23-d5-Trp2 in the Absence and Presence of Cholesterol

cholesterol (mol %) quadrupolar splittingsa (kHz)
18 38 57
90° 9 19 29 41
4 15 40 60
90° 4 6 20 30 39
a

The quadrupolar splittings are estimated to have an experimental error of 1−2 kHz (compare to ref 48).