Scheme 6a.
a Reagents and conditions: (a) Ph2SO, Tf2O, TBP, CH2Cl2; 43 (55%); (b) 41, Ph2SO, Tf2O, TBP, CH2Cl2; add 52 (88%); (c) TBAF, THF (98%); (d) Ph2SO, Tf2O, TBP, CH2Cl2; add 51 (85%); (e) K2CO3, MeOH (91%).
a Reagents and conditions: (a) Ph2SO, Tf2O, TBP, CH2Cl2; 43 (55%); (b) 41, Ph2SO, Tf2O, TBP, CH2Cl2; add 52 (88%); (c) TBAF, THF (98%); (d) Ph2SO, Tf2O, TBP, CH2Cl2; add 51 (85%); (e) K2CO3, MeOH (91%).