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NMR data at pH 6 for PP-IP5
| Position | δH | 3JH-Ha | δP | 3JP-Hb | 2JP-Pb |
|---|---|---|---|---|---|
| ppm | Hz | ppm | Hz | Hz | |
| 1/3 | 4.286 | 2.4, 9.3 | 1.412 | 9.5 | |
| 2 | 5.077 | 2.4 | 0.733 | 9.9 | |
| 3/1α | 4.374 | 2.4, 9.4 | −9.766 | 10.0 | 20.4 |
| 3/1β | −7.954 | 20.4 | |||
| 4/6 | 4.561 | 9.4 | 1.660 | 9.9 | |
| 5 | 4.305 | 9.4 | 2.914 | 10.5 | |
| 6/4 | 4.541 | 9.4 | 1.997 | 9.2 |
Error in coupling constant from one-dimensional 1H NMR data is 0.16 Hz.
Error in coupling constant from one-dimensional 31P NMR data is 0.25 Hz.
