Table 6.
Entry | Amide | Product | Time (min) | Yield (%) |
---|---|---|---|---|
1 | 15 | 92 | ||
2 | 90 | 51 | ||
3 | 30 | 46 | ||
4 | 90 | 57 | ||
5 | a | 10 | 0 | |
6 | 15 | 90 | ||
7 | N.R. | 45 | 0 | |
8 | N.R. | 45 | 0 |
Complete loss of starting material without observation of aldehyde.
Entry | Amide | Product | Time (min) | Yield (%) |
---|---|---|---|---|
1 | 15 | 92 | ||
2 | 90 | 51 | ||
3 | 30 | 46 | ||
4 | 90 | 57 | ||
5 | a | 10 | 0 | |
6 | 15 | 90 | ||
7 | N.R. | 45 | 0 | |
8 | N.R. | 45 | 0 |
Complete loss of starting material without observation of aldehyde.