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. Author manuscript; available in PMC: 2009 Jan 14.
Published in final edited form as: J Am Chem Soc. 2007 Feb 22;129(11):3408–3419. doi: 10.1021/ja066362+

Table 9.

Solvent Effects on Reaction

graphic file with name nihms-61943-t0117.jpg
Entry Solvent Yield (%)a tdissb
1 oxetane 95 2-3
2 tetrahydrofuran 99 15
3 1,4 dioxane 15 -
4 pyridine 15 1
5 toluene 15 -
6 chloroform 0 -
a

Aldehyde yield after 30 min period

b

Time of reagent dissolution in minutes