. Author manuscript; available in PMC: 2009 Sep 1.

Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2008 Jul 31;872(1-2):141–147. doi: 10.1016/j.jchromb.2008.07.032

Table 1.

Assay performance data of the calibration samples for ABT-888 and M8 in human plasma.

Analyte	Concentration (ng/mL)	Accuracy (%)	Intra-assay precision (%)	Inter-assay precision (%)

ABT-888	10	100.4	4.5	-^*
	30	99.9	5.0	-^*
	100	100.6	3.3	-^*
	300	101.0	3.6	2.8
	500	102.4	2.8	2.0
	750	101.6	3.9	-^*
	1000	96.5	3.6	1.7

M8	10	101.4	5.7	-^*
	30	97.4	4.2	2.4
	100	100.8	7.0	-^*
	300	102.3	5.5	-^*
	500	104.6	6.3	-^*
	750	104.4	12.1	-^*
	1000	98.3	11.3	-^*

N=9; triplicate results, each in 3 separate runs, for each concentration.

The mean square of the within runs was greater than the mean square of the between runs, indicating that there was no significant additional variation due to the performance of the assay in different runs [9].