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. Author manuscript; available in PMC: 2009 Apr 9.
Published in final edited form as: J Am Chem Soc. 2008 Mar 13;130(14):4859–4868. doi: 10.1021/ja7100642

Figure 13.

Figure 13

Selected 6Li NMR spectra from solvent swap experiments using 0.10 M [6Li]1 with 3.0 M total ligand/toluene at -90 °C. A) Solvent swap between THF and DME. The mixed solvate is observed at 1:30 ratio of the two solvents. B) Solvent swap between THF and TMEDA. Both aggregation states are observed at a solvent ratio of 1:2.