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. Author manuscript; available in PMC: 2010 Jan 14.
Published in final edited form as: J Am Chem Soc. 2009 Jan 14;131(1):12–13. doi: 10.1021/ja805521y

Figure 3.

Figure 3

13C-13C TOCSY NMR spectrum of [2H7, 13C6]-glucose solution, with DNP (10 s)-TJ (0.8 s) and 40 s recycle delay. 1 transient of 1024 data points was accumulated for 96 t1 increments. 4.5 ms of DIPSI-2 mixing with ω1/2π = 29 kHz was used for TOCSY. The 2D data matrix was acquired with 2 * 96 * 1024 points, with a single transient per data file and a recycle time of 40 s required by the refreezing. 2H decoupling was applied in both dimensions.