TABLE 1.
Data collection and refinement statistics
| Data collection | |
| Resolution (Å) | 30-2.5 (2.6-2.5)a |
| Rsym | 9.7 (49.3) |
| <I / σI> | 6.8 (2.1) |
| Completeness (%) | 99.8 (100) |
| Unique/observed reflections | 43749/285072 (4650/20528) |
| Wilson B-factor (Å2) | 51 |
| Refinement | |
| Resolution (Å) | 30-2.5 (2.6-2.5) |
| Rwork/Rfree | 24.3/26.8 (38.2/41.4) |
| r.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 1.28 |
| Average B-factors (Å2) | 35.8 |
| Ramachandran plotb: favored, allowed (%) | 98.2, 1.8 |
a
Values in parentheses are for highest-resolution shell.
b
According to Molprobity (20).