TABLE 2. LC/MS/MS Method Performance Characteristics for PbTx Analysis.
linerarity, R2 | accuracy (% deviation) |
% recovery | precision, CVa (%) | LOQb (ng/sample) |
|
---|---|---|---|---|---|
PbTx1 | 0.99 | 13 | 27 | 11 | 0.6 |
PbTx2 | 0.99 | 5 | 54 | 6 | 0.4 |
PbTx3 | 0.99 | 9 | 66 | 9 | 0.4 |
PbTx6 | 0.99 | 15 | 59 | 7 | 0.4 |
PbTx9 | 0.99 | 7 | 61 | 10 | 0.4 |
brevenal | 0.99 | 12 | 35 | 12 | 0.4 |
Coefficient of variation.
Limit of quantitation.
The analyses were performed at the concentration range of 0.8–500 ng/mL.