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. Author manuscript; available in PMC: 2009 Mar 9.
Published in final edited form as: Environ Sci Technol. 2005 May 15;39(10):3443–3449. doi: 10.1021/es048680j

TABLE 2. LC/MS/MS Method Performance Characteristics for PbTx Analysis.

linerarity, R2 accuracy
(% deviation)
% recovery precision, CVa (%) LOQb
(ng/sample)
PbTx1 0.99 13 27 11 0.6
PbTx2 0.99 5 54 6 0.4
PbTx3 0.99 9 66 9 0.4
PbTx6 0.99 15 59 7 0.4
PbTx9 0.99 7 61 10 0.4
brevenal 0.99 12 35 12 0.4
a

Coefficient of variation.

b

Limit of quantitation.

c

The analyses were performed at the concentration range of 0.8–500 ng/mL.