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. Author manuscript; available in PMC: 2009 Dec 3.
Published in final edited form as: J Am Chem Soc. 2008 Dec 3;130(48):16262–16273. doi: 10.1021/ja8044986

Table 1.

Crystal structure parameters of L1 and L3 complexes. All distances are in angstroms and all angles in degrees.

Parameter L1 L3
Cu-O 1.731(3) 1.837(2)
Cu-N4 2.043(4) 2.085(3)
Cu-N6 1.995(4) 1.931(2)
Cu-N8 2.023(3) 2.046(2)
Cu-O-C 138.0(4) 126.0(2)
O-Cu-N4 120.1(2) 103.20(9)
O-Cu-N6 129.8(2) 161.91(9)
O-Cu-N8 121.1(1) 103.30(9)
N4-Cu-N6 90.9(1) 87.0(1)
N4-Cu-N8 92.5(1) 109.48(9)
N6-Cu-N8 92.9(1) 86.87(9)