TABLE 1.
Data collection and refinement statistics for C. japonicus Man26C
| Apo-CjMan26C | CjMan26C-mannose | E338A CjMan26C-mannobiose | CjMan26C-6163-Gal2Man4 | |
|---|---|---|---|---|
| Data collection | ||||
| Space group | P212121 | P6122 | P6122 | P6122 |
| Cell dimensions (Å) | 52.3, 83.6, 84.3 | 84.7, 84.7, 244.7 | 84.3, 84.3, 243.3 | 84.5, 84.5, 244.3 |
| Resolution (Å) | 20-1.7 (1.76-1.70) | 50-1.47 (1.52-1.47) | 20-1.80 (1.86-1.80) | 20-1.57 (1.63-1.57) |
| Rmerge (%) | 8.3 (48.6) | 5.8 (28.7) | 8.7 (41.1) | 6.2 (24.6) |
| I/σI | 19.4 (3.7) | 47.4 (5.3) | 16.2 (2.9) | 38.4 (10.4) |
| Completeness (%) | 100 (100) | 99.1 (91.7) | 99.9 (100) | 99.4 (99.3) |
| Redundancy | 7.0 (7.0) | 9.1 (7.0) | 9.5 (8.8) | 11.3 (11.0) |
| Refinement | ||||
| Rwork/Rfree | 16/19 | 13/16 | 16/18 | 12/15 |
| Root mean square deviation bond lengths (Å) | 0.004 | 0.012 | 0.015 | 0.009 |
| Root mean square deviation bond angles (degrees) | 0.6 | 0.9 | 1.3 | 0.9 |