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. Author manuscript; available in PMC: 2009 Apr 7.
Published in final edited form as: Langmuir. 2008 Aug 23;24(19):10621–10624. doi: 10.1021/la801645x

Figure 1.

Figure 1

(a) Initially, a drop of the crystalline mesophase is deposited on a clean, empty rivet that is held in place on the cryo-sample stage at room temperature. (b) The sample stage with the crystalline mesophase is immediately frozen in slushed liquid nitrogen and transferred under vacuum to the cryo-SEM. (c) The sample is subsequently fractured to reveal a clean surface that is then sublimed and sputter coated with platinum prior to imaging.