Table 2.
Data collection and refinement statistics
| Crystal gp18PR, SeMet derivative | Crystal gp18 M | |
|---|---|---|
| Data collection | ||
| Space group | F432 | C2221 |
| Cell dimensions | ||
| a, b, c (Å) | 203.66 | 99.591 |
| 203.66 | 116.288 | |
| 203.66 | 433.759 | |
| α, β, γ (deg) | 90, 90, 90 | 90, 90, 90 |
| Resolution (Å) | 50 (1.8)a | 50 (3.5) |
| Rmerge | 6.4 (79.4) | 10.6 (29.1) |
| I/ΔI | 26.8 (2) | 11.9 (3.2) |
| Completeness (%) | 96.6 (95.5) | 87.1 (61.1) |
| Redundancy | 5.5 (4.4) | 3.7 (2.7) |
| Refinement | ||
| Resolution (Å) | 36 (1.8) | 50 (3.5) |
| No. of reflections | 55815 | 28369 |
| Rwork/Rfree | 18.98/21.94 | 26.54/29.86 |
| R.m.s. deviations | ||
| Bond length (Å) | 0.005 | 0.006 |
| Bond angle (deg) | 1.013 | 1.054 |
| aValues in parentheses are for highest-resolution shell. | ||