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Comparison of ηz rates determined from the ηz∕κ experiment described here and the PFB experiment described by Pelupessy et al. (Ref. 21). Sample consists of 2.0 mM 15N-labeled protonated human ubiquitin in 90∕10% H2O∕D2O at pH 4.8 and 30.0 °C. Instrument: Bruker AMX 500, no cryo probe.
