Table 1. Crystallographic data collection and structure solution.
Data collection | |
Resolution range (Å) | 20.0-1.45 (1.49-1.45) |
Space group | P21 |
Unit cell dimensions | |
a, b, c (Å) | 65.3, 81.3, 71.2 |
α, β, γ (°) | 90.0, 111.3, 90.0 |
Completeness (%) | 98.9 (98.7) |
Rsym (%) | 6.5 (57.5) |
Redundancy | 4.0 (3.6) |
<I/σ(I)> | 8.9 (2.7) |
Refinement | |
Resolution range (Å) | 10.0-1.45 |
Rcryst (%) | 18.4 |
Rfree (%) | 21.6 |
Rmsd bond lengths (Å) | 0.020 |
Rmsd bond angles (°) | 1.8 |
Rmsd B factors of bonded atoms (main chain, side chain) (Å2) | 2.5, 4.8 |
Ramachandran plot (%) | |
Preferred | 97.8 |
Allowed | 2.2 |
Outliers | 0.0 |