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. 2009 Apr 28;65(Pt 5):522–525. doi: 10.1107/S1744309109013979

Phasing took place with two derivatives by MIRAS using SOLVE in the resolution range 3.50–20.00 Å. All data sets were collected on SLS beamline PXII and were combined with CAD and scaled with SCALEIT prior to use in SOLVE.

Phasing set Native TAMM CsCl
Radiation source SLS PXII SLS PXII SLS PXII
Preparation 24 h soak, 10 mM in cryosolution 20 min soak, 200 mM in cryosolution
Heavy-atom location method INANO, ANOREFINE INANO, NOANOREFINE
Phasing power (acentric/centric) 1.48/1.11 0.73/0.56
Figure of merit (all data) 0.29 0.29