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Typical example of the paramagnetic effects on TOCSY Spectra. The aromatic region of 3 with DPC micelles (left column), with 200 μM Mn2+ (middle) and 5-DOXYL stearic acid (right). Preserved resonances (labeled) are in a phase not missed by the phase-specific radical probe (Mn2+ or DOXYL). Spectra were compared from the same noise level. The full spectra for 1-3 are available in the Supporting Information.
